Electric Literature of 38584-37-1 , The common heterocyclic compound, 38584-37-1, name is 3-(Hydroxymethyl)adamantan-1-ol, molecular formula is C11H18O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
(3) Esterification and polymerization A mixture of 1-hydroxy-3-hydroxymethyladamantane (1 mmol), acryloyl chloride (1.2 mols), triethylamine (1.2 mols) and dioxane (10 ml) was stirred at 40C for 3 hours. As a result, 1-hydroxy-3-(acryloyloxymethyl)adamantane of the following formula was obtained (yield 90%).
The synthetic route of 38584-37-1 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Daichel Chemical Industries Ltd; EP1000924; (2000); A1;,
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