Category: 10213-78-2

Synthetic Route of 10213-78-2, Adding some certain compound to certain chemical reactions, such as: 10213-78-2, name is 2,2′-(Octadecylazanediyl)diethanol,molecular formula is C22H47NO2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 10213-78-2.

EXAMPLE V Preparation of Methylbis(2-hydroxyethyl)octadecyl Ammonium Methyl Sulfate in Polyoxyethylene(5)glycoloctadecanoate To 150 g (0.418 gmol) of bis(2-hydroxyethyl)octadecylamine in 203 g of polyoxyethylene(5)glycoloctadecanoate heated to 75 C. with stirring in a 1-liter, 3-neck glass round-bottom flask fitted with a thermometer and electric heating mantle there was added 51.1 g (0.405 gmol) of dimethyl sulfate (Aldrich, 99%). The temperature rose immediately to 120 C.; the heat was removed and the reaction mixture allowed to cool to 35-40 C. at which solidification began to occur. A sample of the mixture analyzed as 48% quaternary, 2.16% amine methylsulfate and 1.67% amine and amine soap, calculated as amine.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 10213-78-2, 2,2′-(Octadecylazanediyl)diethanol, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Akzona Incorporated; US4237064; (1980); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Electric Literature of 10213-78-2 ,Some common heterocyclic compound, 10213-78-2, molecular formula is C22H47NO2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

In a 250 ml Erlenmeyer flask, 13 g (36 mmol) of N-octadecylamine in 100 ml of chloroform was dissolved and cooled to 0 C. Then, 7.95 ml (0.109 mol) of thionyl chloride was added dropwise to the cooled material. After completion of the addition, the reaction mixture was heated under chloroform reflux for 3 hours. An excess of the solvent and thionyl chloride were evaporated, and the residue taken up in dichloromethane was washed with Na2CO3 saturated solution, and washed several times with water until neutralization. The organic phase was dried over MgSO4, filtered, and concentrated under vacuum. The residue was purified by chromatography on a silica gel column using an ether/petroleum ether mixture (5:95 v/v) as eluent. This yielded 10 g of pure amine chloride as oil. Yield: 70%. Rf: 0.43 (ether/petroleum ether, 5:95 v/v). 1H NMR (200 MHz, CDCl3, HMDS) delta ppm: 3.38 (t, 4H, J=5.43 Hz, CH2-Cl), 2.75 (t, 4H, J=7.30 Hz, N-CH2-C-Cl), 2.43 (t, 2H, J=6.67 Hz, CH2-N), 1.36 (m, 2H, CH2-C-N), 1.16 (s1, 30H, CH2), 0.80 (t, 3H, J=5.85 Hz, CH3).

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,10213-78-2, its application will become more common.

Reference:
Patent; Yang Ji Chemical Company Ltd.; US2005/75345; (2005); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

10213-78-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 10213-78-2, name is 2,2′-(Octadecylazanediyl)diethanol, molecular formula is C22H47NO2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

In a two-necked flask equipped with 35.8 g of N, N-dihydroxyethyl octadecylamine, 13.3 g of DMT0 and 6.2 g of boric acid , The reaction was carried out for 8 hours. After the completion of the reaction, the organic solvent was removed under reduced pressure to obtain 38.6 g of a reddish brown viscous compound of the hydroxyalkylated heterocyclic borate ester with BPTT as the main product Liquid, the yield of 100%. The total yield was 74.35%.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 10213-78-2, 2,2′-(Octadecylazanediyl)diethanol, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Shanghai Jiao Tong University; Li, Zhipeng; Zhang, yawen; Li, Jianchang; Ren, Tianhui; (22 pag.)CN103601748; (2016); B;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts