Introduction of a new synthetic route about 10213-78-2

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 10213-78-2, 2,2′-(Octadecylazanediyl)diethanol, other downstream synthetic routes, hurry up and to see.

10213-78-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 10213-78-2, name is 2,2′-(Octadecylazanediyl)diethanol, molecular formula is C22H47NO2, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

In a two-necked flask equipped with 35.8 g of N, N-dihydroxyethyl octadecylamine, 13.3 g of DMT0 and 6.2 g of boric acid , The reaction was carried out for 8 hours. After the completion of the reaction, the organic solvent was removed under reduced pressure to obtain 38.6 g of a reddish brown viscous compound of the hydroxyalkylated heterocyclic borate ester with BPTT as the main product Liquid, the yield of 100%. The total yield was 74.35%.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 10213-78-2, 2,2′-(Octadecylazanediyl)diethanol, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Shanghai Jiao Tong University; Li, Zhipeng; Zhang, yawen; Li, Jianchang; Ren, Tianhui; (22 pag.)CN103601748; (2016); B;,
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