Category: 92409-15-9

Synthetic Route of 92409-15-9, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 92409-15-9, name is 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol. This compound has unique chemical properties. The synthetic route is as follows.

1 part by weight of the compound2- (2-methoxyphenoxy) -1- (4-methoxyphenyl) -1-hydroxy-3-propanol and 1.8 parts by weightAl (NO3) 3 was added to 30 parts by weight of methanol,Set the microwave reactor power of 50W,Microwave frequency of 2450MHz, microwave-assisted heating at 80 for 40min.After completion of the reaction, the reaction was quenched with cold water immediately,The reaction solution was extracted with ethyl acetate,Take organic phase spin dry,Followed by further separation and purification by silica gel column chromatography,The mobile phase of ethyl acetate and n-hexane volume ratio of 1: 1, evaporated to dry the solvent that methylation products.

According to the analysis of related databases, 92409-15-9, the application of this compound in the production field has become more and more popular.

Reference:
Patent; South China University of Technology; Qiu, Xueqing; Ouyang, Xinping; Zhu, Guodian; Chen, Cheng; Jin, Dongxue; Zhao, Ying; (10 pag.)CN106117021; (2016); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Reference of 92409-15-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 92409-15-9, name is 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol, molecular formula is C17H20O5, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

The 152 mg type g shown in lignin of beta – O – 4 model compound, 8 mg double rhodium catalyst, 80 mg NaOH added 1 ml distilled water, under protection of argon 110 C reaction 18 hours, to complete the lignin complete degradation, wherein the degradation product to the methoxy acetophenone of yield is 24%, P-acetone to yield 34%, O-methoxyphenol of yield is 62%.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 92409-15-9, 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol.

Reference:
Patent; Shaanxi Normal University; Dalian Institute of Chemical Physics; Wang Chao; Liu Yuxuan; Li Changzhi; Xiao Jianliang; Wang Aiqin; Zhang Tao; Li Junjun; Xue Dong; Tang Weijun; (9 pag.)CN107253904; (2017); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Electric Literature of 92409-15-9 ,Some common heterocyclic compound, 92409-15-9, molecular formula is C17H20O5, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.

General procedure: The catalytic hydrogenolysis of lignin model compounds was performedusing a 50 mL Zr-alloy autoclave provided by Anhui KemiMachinery Technology Co., Ltd. For a typical procedure, lignin modelcompounds (0.5 mmol or 1 mmol) or organosolv lignin (35 mg), heterogeneousFe catalyst (100 mg), and solvent (20 mL) were added intothe autoclave with a quartz lining. After purging the reactor with H2,the reaction was conducted with 1 MPa H2 (at room temperature) at240 C for 12 h with a stirring speed of 800 rpm. After reaction, internalstandards are added to the product solution, and then the liquid productswere analyzed by using both GC and GC-MS. For the conversionof alpha-O-4 lignin model compound, 2-phenylethanol is used as internalstandard to determine the yields of benzyl alcohol and phenol, anddodecane is used to determine the yield of toluene. For the conversionof beta-O-4 lignin model compounds, benzyl alcohol and dodecane areused as internal standards to determine the yields of phenolic fragmentsand aromatic fragments, respectively. A representative GC spectrumcan be seen in Fig. S11 in supporting information. GC-MS analyses wereperformed on an Agilent 7890 Gas Chromatograph equipped with a DBWAXETR30m×0.25 mm×0.25mm capillary column (Agilent) or aHP-5MS 30m×0.25 mm×0.25mm capillary column (Agilent).Although HP-5MS column is unsuitable for the determination of productsyields due to the low polarity, it can be used to confirm whethersome complex lignin model compounds were completely converted.The GC was directly interfaced to an Agilent 5977 mass selective detector(EI, 70 eV). The following GC oven temperature programs wereused: 40 C hold for 1 min, ramp 5 C min-1 to a temperature of 120 C,and then ramp 10 C min-1 to 300 C and hold for 5 min. To get the representative GC spectrum of gaseous products, the gaseous phase wascollected and injected into a Fuli 9790II Gas Chromatograph equippedwith a TDX-01 packed column and a thermal conductivity detector(TCD) through a six-way valve to analyze the composition.

These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,92409-15-9, its application will become more common.

Reference:
Article; Li, Jiang; Sun, Hui; Liu, Jia-xing; Zhang, Jun-jie; Li, Zhen-xing; Fu, Yao; Molecular catalysis; vol. 452; (2018); p. 36 – 45;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Application of 92409-15-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 92409-15-9, name is 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol, molecular formula is C17H20O5, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

In 5 ml of quartz optical reaction tube, adding 0.05 mmol 2-(2-methoxyphenoxy)-1-(4-methoxyphenyl)-1,3-propanediol, 5 mg mpg-C3N4Catalyst, magneton, and add 1 ml solvent acetonitrile (substrate concentration is 0.05 mol/L). Air above the oxygen displacement reaction tube, and the opening is sealed, is arranged in the integrated light in the reaction device, the rotating speed of 500 r/min, the illumination wavelength is 405 nm (the power of 6 W), temperature constant at 40C, reaction 8 h. After the reaction, gas chromatography – mass spectrum detecting the product, and for high performance liquid chromatography quantitative, substrate conversion and product yield is shown in table 1.

According to the analysis of related databases, 92409-15-9, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Dalian Institute of Chemical Physics; Wang Feng; Liu Huifang; Wang Min; Li Hongji; Luo Nengchao; Su Kaiyi; (14 pag.)CN109456160; (2019); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts

Related Products of 92409-15-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 92409-15-9, name is 2-(2-Methoxyphenoxy)-1-(4-methoxyphenyl)propane-1,3-diol, molecular formula is C17H20O5, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

In 5 ml of quartz optical reaction tube, adding 0.05 mmol 2-(2-methoxyphenoxy)-1-(4-methoxyphenyl)-1,3-propanediol, 5 mg mpg-C3N4Catalyst, magneton, and add 1 ml solvent acetonitrile (substrate concentration is 0.05 mol/L). Air above the oxygen displacement reaction tube, and the opening is sealed, is arranged in the integrated light in the reaction device, the rotating speed of 500 r/min, the illumination wavelength is 405 nm (the power of 6 W), temperature constant at 40C, reaction 8 h. After the reaction, gas chromatography – mass spectrum detecting the product, and for high performance liquid chromatography quantitative, substrate conversion and product yield is shown in table 1.

According to the analysis of related databases, 92409-15-9, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Dalian Institute of Chemical Physics; Wang Feng; Liu Huifang; Wang Min; Li Hongji; Luo Nengchao; Su Kaiyi; (14 pag.)CN109456160; (2019); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts