Related Products of 2576-29-6, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 2576-29-6, name is 2-((2-Chloroethyl)amino)ethanol hydrochloride, molecular formula is C4H11Cl2NO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Similarly, a suspension of 2-[(2-chloroethyl)amino]ethanol hydrochloride (2.0 g, 8.4 mmol) in 1,4-dioxane (150 mL) was treated with Et3N (1.8 g), cooled with ice bath and then 15 (2.0 g,5.4 mmol) was added. The reaction was kept at 20 0C overnight, then water (100 mL) was added and the mixture was extracted with EtOAc (3×150 mL). The combined organic phases were washed with pre-cooled dilute HCl, water, aqueous NaHCO3, and brine, dried and concentrated under pressure, and then passed through a short column of silica gel, eluting with heptane/EtOAc (1:1), to give 16a (4.1 g, 37%).
According to the analysis of related databases, 2576-29-6, the application of this compound in the production field has become more and more popular.
Reference:
Patent; AUCKLAND UNISERVICES LIMITED; WO2008/30112; (2008); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts