Related Products of 39067-45-3, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 39067-45-3, name is 3-(Diethylamino)-2,2-dimethylpropan-1-ol. This compound has unique chemical properties. The synthetic route is as follows.
EXAMPLE III 3-Diethylamino-2,2-dimethylpropyl 3,4-dimethoxyphenylcinnamate hydrochloride 3,4-Dimethoxycinnamic acid (31.4 g, 0.15 mole) was added with rapid stirring to thionyl chloride (52.5 ml) and refluxed for 4 hours. The mixture was stripped of excess thionyl chloride under reduced pressure, benzene (100 ml) was added, and the mixture was again stripped of solvent. The residue was treated with a solution of 3-diethylamino-2,2-dimethylpropanol (24.2 g, 0.15 mole) in benzene (500 ml), refluxed for 3 hours, cooled, diluted with petroleum ether (500 ml), and stored overnight at room temperature. The benzene-petroleum ether solution was decanted, the residue dissolved in H2 O (800 ml), and the solution adjusted to pH 8 with saturated aqueous K2 CO3 (60 ml). The product was extracted from the aqueous phase with benzene (800 ml) in portions and the extract dried overnight over MgSO4 and Darco. The solution was filtered and the filtrate adjusted to pH 3 with a solution of dry HCl in ether (cooled in ice bath). Petroleum ether (500 ml) was added and the product oiled out of solution. The benzene-petroleum ether solution was decanted, chloroform (5-0 ml) was added and the mixture was stripped to dryness under reduced pressure. This procedure was repeated three times and then the residue was washed with anhydrous ether (scratching induced crystallization). The product was collected by filtration, yield: 34 g (59%). A sample was recrystallized from ethyl acetate, m.p. 135-138. Anal. Calc’d for C20 H31 NO4.HCl: C, 62.24; H, 8.36; N, 3.63. Found: C, 62.43; H, 8.37; N, 3.62.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 39067-45-3, 3-(Diethylamino)-2,2-dimethylpropan-1-ol.
Reference:
Patent; Morton-Norwich Products, Inc.; US3946042; (1976); A;,
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