Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 624-95-3, name is 3,3-Dimethylbutan-1-ol. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 624-95-3
In a 1 L round bottom flask equipped with a reflux condenser, 232 g of concentrated sulfuric acid and 283 g (48% aqueous solution) of hydrobromic acid were added to 100 g (0.98 mol) of 3,3-dimethyl-1-butanol while cooling in an ice bath did. The mixture was refluxed for 6 hours, cooled to room temperature and then added to 400 g of ice. The aqueous phase was extracted with 400 ml of pentane. The organic phase was washed with 2 M NaOH solution and water, dried over magnesium sulfate and the solvent was removed in vacuo. The product was distilled in vacuo to give 88.1 g (55%) of 1-bromo-3,3-dimethyl-butane as a colorless oil.
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Reference:
Patent; LUMMUS NOVOLEN TECHNOLOGY GMBH; (91 pag.)JP6196581; (2017); B2;,
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