Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3840-31-1, name is (3,4,5-Trimethoxyphenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. HPLC of Formula: C10H14O4
A mixture of 15 g (75.76 mmol) of alcohol 8,7.5 g (113.6 mmol) of 85% potassium hydroxide, and120 mL of DMSO was heated at 110-120 in arotating pressure reactor of 1 liter capacity at acetylenepressure of 1012 atm for 5 h. The mixture was dilutedwith 300 mL of water, the reaction product wasextracted into ethyl acetate (4 × 50 mL). The organic phase was washed with water, dried with Na2SO4, thesolvent was distilled off. To purify the residue it waspassed through a small bed of alkaline alumina (eluentether). Yield 15.45 g (91%), yellowish liquid. 1 NMRspectrum, delta, ppm: 3.73 s (3, OCH3), 3.75 s (6,OCH3), 4.00 d (1, =CH2, 3J 6.8 Hz), 4.22 d (1,=CH2, 3J 14.3 Hz), 4.58 s (2, OCH2), 6.456.52 m (3,=CH, Carom). 13 NMR spectrum, delta, ppm: 55.75(OCH3), 60.05 (OCH3), 69.95 (OCH2), 87.22 (=CH2),106.81 (Carom), 132.32 (Carom), 138.16 (Carom),151.61 (=CH), 153.51 (Carom). Found, %: 64.54; 7.35. C12H16O4. Calculated, %: 64.27; 7.19.
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Reference:
Article; Potapov; Panov; Musalov; Zhivet?eva; Musalova; Khabibulina; Amosova; Russian Journal of Organic Chemistry; vol. 52; 11; (2016); p. 1571 – 1575; Zh. Org. Khim.; vol. 52; 11; (2016); p. 1579 – 1583,5;,
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