Analyzing the synthesis route of 13588-28-8

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 13588-28-8, 2-(2-Methoxypropoxy)propan-1-ol.

Related Products of 13588-28-8, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 13588-28-8, name is 2-(2-Methoxypropoxy)propan-1-ol. This compound has unique chemical properties. The synthetic route is as follows.

Jimroth type reflux condenser, Dean-Stark trap tube,In a 100 mL two-necked flask equipped with a nitrogen inlet tube,Dipropylene glycol monomethyl ether represented by the following formula (20) (with isomer) (7.41 g, 50 mmol), vinylacetic acid synthesized in Example 1 (formula (1-0),4.74 g, 55 mmol),p-Toluenesulfonic acid monohydrate (0.48 g, 2.5 mmol)And toluene (35 mL) was added.Immerse the two-necked flask in an oil bath,The temperature of the oil bath was raised to 130 C.While maintaining the same temperature, the mixture was stirred for 4 hours under a nitrogen stream to distill off the by-produced water.Cool the two-necked flask to room temperature (25 C),Wash twice with 5 wt% aqueous sodium bicarbonate (10 mL),Further, after washing twice with distilled water (10 mL), it was dried over magnesium sulfate. After removing the magnesium sulfate, the solution was concentrated under reduced pressure in the same manner as in Example 2. The obtained concentrated residue was purified by distillation under reduced pressure to isolate the compound (1-1b) (10.57 g, yield 98%)

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 13588-28-8, 2-(2-Methoxypropoxy)propan-1-ol.

Reference:
Patent; JNC Corporation; Masayuki, Sato; Urata, Yasuo; Yatsuda, Shinichi; Masuhara, Shigeo; Hashimoto, Kazuki; (20 pag.)JP5803424; (2015); B2;,
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