Sep 2021 News Extended knowledge of 1562-00-1

According to the analysis of related databases, 1562-00-1, the application of this compound in the production field has become more and more popular.

Reference of 1562-00-1, Adding some certain compound to certain chemical reactions, such as: 1562-00-1, name is Sodium isethionate,molecular formula is C2H5NaO4S, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1562-00-1.

Example 4; Preparation of [C2dmim][ise]; [C2dmim][ise] is an IL comprised of 1-ethyl-2,3-dimethylimidazolium as the cation, and isethionate (ise) as the anion. A 250-mL round bottom flask was charged with [C2dmim]2[SO4] (7.331 g, 21 mmol) and 2:1 alcohol-water (24 mL). This mixture was stirred until forming a clear, colorless solution, whereupon a prepared solution of sodium isethionate (6.267 g, 42 mmol) was added to the mixture in one portion with stirring. A fine precipitate formed soon thereafter. The resulting slurry was stirred for about 2 h, whereupon it was suction filtered, and the filtrate was concentrated as far as feasible by rotary evaporation. The residue was taken up in methanol (25 mL) and loaded onto an about 20-g column of 230-400 mesh silica gel previously packed in methanol.As in Example 3, the methanolic solution of crude [C2dmim][ise] was pushed down to the level of the top of the silica gel bed with air pressure while the column issue was collected in a 250-mL round bottom flask; the flask previously containing the crude product was rinsed with methanol (25 mL) and the rinse methanol was similarly loaded and pressed down while the column issue was collected on top of the first fraction. The rinsing process was repeated once before the silica gel column was washed down with fresh methanol (100 mL), all the while collecting the column issue on top of the accumulated methanol solution. The combined methanolic fractions were concentrated by rotary evaporation to produce purified [C2dmim][ise] (10.713 g, 43 mmol, 101%) as an ionic liquid. The ionic liquid of Example 4 was liquid at ambient conditions.

According to the analysis of related databases, 1562-00-1, the application of this compound in the production field has become more and more popular.

Reference:
Patent; FLUIDIC, INC.; US2012/321967; (2012); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts