Reference of 767-90-8, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 767-90-8, name is (2-Ethylphenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows.
To a solution of (2-ethylphenyl)metha- nol (13-1, 1.00 g, 7.3 mmol) in DMF (25 mE) at room temperature under nitrogen, N135 (2.6 g, 14.6 mmol) and triphenylphosphine (4.03 g, 15.3 mmol) were added sequentially. The mixture was heated to 50 C. overnight, cooled to room temperature and diluted with water and dichloromethane. The aqueous layer was extracted twice more with dichioromethane and the organic layers were combined, washed with brine, dried, filtered and concentrated. The residue was purified by silica gel column chromatography, eluting with 10% ethyl acetate in hexanes to give 1-(bromomethyl)-2-ethylbenzene (13-2, 1.1 g) as an oil.
According to the analysis of related databases, 767-90-8, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Aviara Pharmaceuticals, Inc.; Biediger, Ronald J.; Benish, Michele A.; Market, Robert V.; Savage, Michael M.; Young, Brandon M.; (49 pag.)US2018/312498; (2018); A1;,
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