In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 616-29-5, name is 1,3-Diaminopropan-2-ol, the common compound, a new synthetic route is introduced below. category: alcohols-buliding-blocks
Preparation of (3-tert-Butoxycarbonylamino-2-hydroxy-propyl)-carbamic Acid Tert-Butyl Ester: To a solution of 1,3 diamino-2-hydroxypropane (10 g, 0.11 mol) in methanol (500 ml) was added di-tert-butyl dicarbonate (48 g, 0.22 mumol) and the reaction stirred for 2 hours at room temperature under a N2 atmosphere. The mixture was concentrated to afford the product as a light yellow oil (31.9 g, 100%). 1H-NMR (CD3OD) delta 1.44 (s, 18H), 3.10 (m, 4H), 3.63 (m, 1H).
The synthetic route of 616-29-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Bridger, Gary; Kaller, Al; Harwig, Curtis; Skerlj, Renato; Bogucki, David; Wilson, Trevor R.; Crawford, Jason; McEachern, Ernest J.; Atsma, Bem; Nan, Siqiao; Zhou, Yuanxi; Schols, Dominique; Smith, Christopher D.; Di Fluri, Maria R.; US2004/19058; (2004); A1;,
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