Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 18068-06-9, name is 4-Methoxycyclohexanol. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 18068-06-9
The residue was dissolved in DCM (2.0 ml_), cooled to 0 C under nitrogen atmosphere, and then methanesulfonyl chloride (0.18 ml_, 2.39 mmol) and triethylamine (0.42 ml_, 2.98 mmol) were added succesively. The reaction mixture was stirred at 0 C for 1 h, and then quenched with water (20 ml_). The aqueous layer was extracted with DCM (3 x 10 ml_). The organic extracts were combined, filtered over a hydrophobic fit and concentrated under reduced pressure to provide (4- methoxycyclohexyl) methanesulfonate (320 mg, 1 .55 mmol, 78% yield) as a yellow oil.
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Reference:
Patent; REDX PHARMA PLC; GUISOT, Nicolas; (191 pag.)WO2017/46604; (2017); A1;,
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