Electric Literature of 1450754-41-2, Adding some certain compound to certain chemical reactions, such as: 1450754-41-2, name is 2-(3-But-3-ynyl-3H-diazirin-3-yl)-ethanol,molecular formula is C7H10N2O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1450754-41-2.
(f) Imidazole (740 mg, 10.87 mmol, 3.0 eq), triphenylphosphine (1.05 g, 3.99 mmol, 1.1 eq) and dichloromethane (5 ml) were added to the reaction flask and cooled to 0 C.Add iodine (1.1 g, 4.35 mmol, 1.2 eq), and add the incubation reaction for 30 minutes.A solution of compound 5 (500 mg, 3.62 mmol, 1 eq) in dichloromethane (1 ml) was added at low temperature, and the mixture was stirred for 4 hours.Quenched with saturated sodium sulfite solution, extracted with ethyl acetate, dried and dried.Purified by column to obtain 400 mg of compound 6, yield: 46%
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 1450754-41-2, 2-(3-But-3-ynyl-3H-diazirin-3-yl)-ethanol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Suzhouguangdian Biological Technology Co., Ltd.; Ni Runyan; Wang Wei; (8 pag.)CN109369532; (2019); A;,
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