Synthetic Route of 929-06-6, Adding some certain compound to certain chemical reactions, such as: 929-06-6, name is 2-(2-Aminoethoxy)ethanol,molecular formula is C4H11NO2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 929-06-6.
To a round-bottomed flask containing dichloromethane (15 mL), 2-(2-aminoethoxy)ethanol1 (1.580 g, 15.03 mmol) was added. The solution was kept in ice bath (0 C). A dichloromethanesolution (9 mL) containing di-tert-butyl dicarbonate (3.726 g, 17.07 mmol) was added dropwise (25 min)to the round-bottomed flask. The progress of this amine protection reaction could be convenientlymonitored using TLC. The reaction was carried out at room temperature for 6.5 h.After the reaction, the mixture was washed first with 10 wt% citric acid (10 mL), then10 wt% NaHCO3 (10 mL 2), and finally with water (10 mL). The organic layer collected wasdried over anhydrous Na2SO4, filtered and concentrated under reduced pressure. The residuewas purifed by column chromatography (ethyl acetate /hexane = 1:3, v/v) to aord tert-butyl(2-(2-hydroxyethoxy)ethyl)carbamate (2.646 g, 86% yield) as colorless liquid.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 929-06-6, 2-(2-Aminoethoxy)ethanol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Li, Hsin-Yi; Chu, Yen-Ho; Molecules; vol. 25; 1; (2020);,
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