Synthetic Route of 2009-83-8, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 2009-83-8, name is 6-Chlorohexan-1-ol, molecular formula is C6H13ClO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Compound [MA11-1] (50.00 g, 256 mmol) was added to a 2 L four-necked flask,6-chloro-1-hexanol (36.74 g,268 mmol), potassium carbonate (106.2 g, 768 mmol), potassium iodide (21.3 g, 128 mmol),DMF (500 g) was heated at 85C.Reaction tracing by HPLC,After confirming the end of the reaction,The reaction solution was poured into distilled water (3L).Filtration, washing with distilled water,Crude product was obtained.After that, the resulting crude product is washed with methanol and filtered.After drying under reduced pressure, 61.9 g of compound [MA11-2] was obtained (yield 82%).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 2009-83-8, 6-Chlorohexan-1-ol.
Reference:
Patent; Richan Chemical Industry Co., Ltd.; Gongli University Faren Bingku Li University; Hou Tenggengping; Shan Zhineiyangyi; Nan Wuzhi; Ming Mudazai; Wan Daichunyan; Lu Zeliangyi; Gen Mulongzhi; Ying Yetingdannierandongni; Sen Neizhengren; Chuan Yeyongtai; Chuan Yuexihong; Jin Tengruisui; (73 pag.)CN107473969; (2017); A;,
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