In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 13726-17-5, name is (4-Chloro-3-methoxyphenyl)methanol, the common compound, a new synthetic route is introduced below. HPLC of Formula: C8H9ClO2
D. Synthesis of 4-chloro-3-methoxybenzaldehyde To a solution of (4-chloro-3-methoxyphenyl)methan-1-ol (5.08 g, 29.4 mmol) in benzene (120 mL) was added MnO2 (5.65 g, 65 mmol). The reaction mixture was refluxed for 17 hr, chilled, and filtered through Celite, washing the cake with CH2Cl2 (300 mL). The filtrate was concentrated in vacuo to give 4-chloro-3-methoxybenzaldehyde (4.5 g, 89%).
The synthetic route of 13726-17-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Portola Pharmaceuticals, Inc.; US6906063; (2005); B2;,
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