As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 624-95-3, name is 3,3-Dimethylbutan-1-ol, molecular formula is C6H14O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below. Computed Properties of C6H14O
EXAMPLE 11-Comparative Example 2; Example It represents a second reference oxidation reaction under the same conditions as for Example I using the second catalyst system reported in the same source, Tetrahedron Letters, 42 (2001) 6651-6653: 51. Omg of Mn (N03) 2H20 (0. 205mmol), 49. 5mg of Cu (N03) 2. 6H20 (0. 205mmol), 85mg TEMPO (0. 536mmol) are dissolved in glacial acetic acid (7 cc) and the solution transferred into a jacketed glass reactor. The reactor is alternately evacuated and purged with oxygen at least five times and the temperature of the catalyst solution is raised to the target value of 45C under constant stirring of 150ORPM. When the temperature reached 45C, 8200 mg of 3, 3-dimethyl-1-butanol (76. 6mmol) are injected through the septum adapter using a gas tight syringe. The recorded oxygen uptake rate is 0.016mmol 02/min and the GC analysis after 300min reaction time showed traces of the desired 3, 3-dimethyl-l-butanal. The graphical presentation of this reaction is also shown in the same Figure 01, curve 2, NS1029.
With the rapid development of chemical substances, we look forward to future research findings about 624-95-3.
Reference:
Patent; THE NUTRASWEET COMPANY; WO2005/82825; (2005); A1;,
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