Adding a certain compound to certain chemical reactions, such as: 1611-56-9, 11-Bromoundecan-1-ol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, SDS of cas: 1611-56-9, blongs to alcohols-buliding-blocks compound. SDS of cas: 1611-56-9
General procedure: Tetrahydropyranylation reactions were carried out in a round bottom flask equipped with a reflux condenser, a CaCl2 tube and a magnetic stirring bar. To a solution of 1.0 × 10-2 mol of compound 1 in 2.5 mL of the solvent (CPME or 2-MeTHF) were added 1.1 × 10-2 mol (0.93 g, 1.0 mL) of 2,3-dihydropyran (2) and the required amount of the catalyst (3.3 × 10-4 or 3.3 × 10-5 mol; see Table 1 and Schemes 1 and 2). The resulting mixtures were vigorously stirred for the reported time at the reported temperature (Table 1 and Schemes 1 and 2). The crude mixtures were filtered, the solvent evaporated and the crude product analyzed by 1H-NMR spectroscopy to determine the conversion of compound 1, then purified and characterized as reported below.
The synthetic route of 1611-56-9 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Azzena, Ugo; Carraro, Massimo; Modugno, Gloria; Pisano, Luisa; Urtis, Luigi; Beilstein Journal of Organic Chemistry; vol. 14; (2018); p. 1655 – 1659;,
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