New downstream synthetic route of 112-27-6

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 112-27-6, 2,2′-(Ethane-1,2-diylbis(oxy))diethanol, other downstream synthetic routes, hurry up and to see.

Reference of 112-27-6, Adding some certain compound to certain chemical reactions, such as: 112-27-6, name is 2,2′-(Ethane-1,2-diylbis(oxy))diethanol,molecular formula is C6H14O4, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 112-27-6.

triethylene glycol single-ended p-toluenesulfonic acid ester synthesis: lmmol of triethylene glycol into the three-necked burningThe flask was filled with ImmoL pyridine, dissolved in 20 mL of dichloromethane and stirred in an ice bath at 0 C. ImmoL p-toluenesulfonyl chloride dissolved in dichloromethane was slowly added dropwise. After 3 hours, the reaction was washed with hydrochloric acid, and the organic layer was washed with water until the aqueous solution became neutral. Dried over anhydrous sodium sulfate, and separated by column chromatography.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 112-27-6, 2,2′-(Ethane-1,2-diylbis(oxy))diethanol, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Gannan Normal University; Wu, Yongquan; Fan, Xiaolin; Ceng, Guanjie; Wu, Renmiao; Jiang, Tianyu; Li, Yibao; (11 pag.)CN105601675; (2016); A;,
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