The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 112-27-6, name is 2,2′-(Ethane-1,2-diylbis(oxy))diethanol. This compound has unique chemical properties. The synthetic route is as follows. Computed Properties of C6H14O4
Polyethylene glycol (9 g, 60 mmol) was dissolved in 70 mL of toluene,Then, 10.2 mL of 48% HBr aqueous solution was added, heated to reflux,With sodium bicarbonate to absorb the release of gas,The reaction temperature was controlled at 115 C and the reaction was stirred for 3 days.After cooling, the reaction mixture was neutralized with saturated aqueous sodium bicarbonate and then solvent was removed. 30 mL of water was added and extracted with CH 2 Cl 2 (3 × 60 mL).The combined organic phases were dried over anhydrous sodium sulfate, and the organic solvent was stripped to give 5.2 g of compound 15 in 41% yield.
With the rapid development of chemical substances, we look forward to future research findings about 112-27-6.
Reference:
Patent; Shanghai Jiao Tong University; Shen Yumei; Yang Qinglai; Tan Lianjiang; Li Xinhui; Shao Zhifeng; Gong Bing; Li Xiaowei; Liu Yazhi; Zhang Zhen; (35 pag.)CN104725453; (2017); B;,
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