Application of 10029-04-6, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 10029-04-6, name is Ethyl 2-(hydroxymethyl)acrylate. This compound has unique chemical properties. The synthetic route is as follows.
Example 5. To a stirring mixture of monoethyl malonate (5.1 g, 38.6 mmol) , ethyl 2-hydroxylmethyl acrylate (5.02 g, 3.86 mmol), PTSA (50 mg) and hydroquinone (50 mg) , was added toluene (50 mL) and the mixture was refluxed at a temperature of 15O0C to azeotropically remove water.[0079] After cooling, the reaction product was washed consecutively with 30% brine and water, and the organic layer was dried over anhydrous sodium sulfate, filtered and the solvent removed by rotary evaporator. The crude reaction product was purified by vacuum distillation (98- 100C/0.1 mbar) and the ester, C was isolated in 80% yield. 1H NMR (60 MHz, CDCl3) : delta 6.36 (s, IH), 5.87 (s, 1 H), 4.89(s, 2 H), 4.05-4.41 (m, 4 H), 3.43 (s, 2 H), 1.19-1.42 (m, 6 H); FT-IR (film) : 2984.7, 2908.6, 1735.3 (br) , 1640.5, 1513,6, 1447.6, 1332.2, 1145.4, 1031.7, 817.2 cm-1; GC/MS(EI) m/z (%) : 245 (2) [M++ H], 226 (2), 199 (20), 153 (20), 129 (70), 115 (100), 101 (40), 85 (45), 43 (65) .
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 10029-04-6, Ethyl 2-(hydroxymethyl)acrylate.
Reference:
Patent; LOCTITE (R & D) LIMITED; WO2009/53484; (2009); A2;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts