New downstream synthetic route of (2,6-Dimethoxyphenyl)methanol

The synthetic route of 16700-55-3 has been constantly updated, and we look forward to future research findings.

Adding a certain compound to certain chemical reactions, such as: 16700-55-3, (2,6-Dimethoxyphenyl)methanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, Quality Control of (2,6-Dimethoxyphenyl)methanol, blongs to alcohols-buliding-blocks compound. Quality Control of (2,6-Dimethoxyphenyl)methanol

Step A Synthesis of 2,6-dimethoxyphenylmethyl bromide as an intermediate After a mixture of 5.7 grams (0.034 mole) of 2,6-dimethoxyphenylmethanol in 40 mL of concentrated hydrobromic acid was stirred at ambient temperature for about one hour, the reaction mixture was taken up in diethyl ether. Solid sodium chloride was added to the mixture to obtain a phase separation. The organic layer was separated and concentrated under reduced pressure, yielding about 4.7 grams of 2,6-dimethoxyphenylmethyl bromide. This compound was used immediately in the next reaction.

The synthetic route of 16700-55-3 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; FMC Corporation; US5569664; (1996); A;; ; Patent; FMC Corporation; US5639763; (1997); A;,
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