Introduction of a new synthetic route about 2,2-Diphenylethanol

With the rapid development of chemical substances, we look forward to future research findings about 1883-32-5.

The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 1883-32-5, name is 2,2-Diphenylethanol. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 2,2-Diphenylethanol

(3) Preparation of 2,2-diphenylethyl methanesulfonate In a 500 mL three-opening flask, 2,2-diphenyl ethanol (17 g, 86 mmol) was dissolved in 170 mL dichloromethane. To the flask was added triethylamine (13.03 g, 129 mmol). The resulting mixture was stirred at 0 C. for half an hour. To the resulting mixture was slowly added MsCl (11.92 g, 104 mmol) dropwisely. The reaction was conducted at 25 C. After the completion of reaction monitored by TLC, the reaction solution was washed with water thrice. The organic phase was dried over anhydrous sodium sulfate and evaporated to remove the solvent to produce 2,2-diphenylethyl methanesulfonate (23 g) in a yield of 96.78%.

With the rapid development of chemical substances, we look forward to future research findings about 1883-32-5.

Reference:
Patent; XUANZHU PHARMA CO., LTD.; Zhang, Hui; Fan, Mingwei; Sun, Liang; US2014/45896; (2014); A1;,
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