Reference of 1467-84-1, Adding some certain compound to certain chemical reactions, such as: 1467-84-1, name is (trans-4-Aminocyclohexyl)methanol,molecular formula is C7H15NO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1467-84-1.
The reference gathers the precedent 14 of the resulting 1 – (4-chloro-1 – {[ 2 – (trimethyl silicon alkyl) ethoxy] methyl} – 1H-pyrrolo [2,3-b] pyridine-5-yl) prop-2-en-1-one (35.3g, 105mmol) add in order to Japan International disclosed in paragraph 2013/024895 of the recorded reference gathers the precedentb 122 the method obtained (trans-4-amino-cyclohexyl) methanol (16.4g, 126mmol), potassium phosphate (44.7g, 210mmol) and dimethyl sulfoxide (175 ml), in 100-110 C stirring 2 hours 30 minutes. Subsequently, to the cold-discharge 50 C rear, for adding water in the reaction mixture. Filter the resulting solid, after washing with ethyl acetate, dried under reduced pressure, the title compound is obtained as light yellow solid (32.1g, yield 71%).
According to the analysis of related databases, 1467-84-1, the application of this compound in the production field has become more and more popular.
Reference:
Patent; NISSAN CHEMICAL INDUSTRIES, LTD.; WATANABE, TSUNEO; TAKAHASHI, KEIJI; HAYASHI, KEISHI; NAKAMURA, TAKANORI; MINAMI, MASATAKA; KURIHARA, KAZUNORI; YAMAMOTO, AKIO; NISHIMURA, TAKUYA; UNI, MIYUKI; KAMIYAMA, TOSHIHIKO; IWAMOTO, SHUNSUKE; (96 pag.)TW2016/7947; (2016); A;,
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