Reference of 171623-29-3, Adding some certain compound to certain chemical reactions, such as: 171623-29-3, name is (4-Cyclopentylphenyl)methanol,molecular formula is C12H16O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 171623-29-3.
General procedure: Under nitrogen atmosphere, to asuspension of 14-21 (1.0 eq.) in dry CH2Cl2 (2.0 mL), DIPEA (1.2 eq.) was added dropwise.Subsequently, the crude mixture containing the corresponding alkyl-2-oxopyridine-1-carboxylate (1.2eq.) in dry CH2Cl2 (4.0 mL) was added. The reaction mixture was stirred at room temperature for 16 h,diluted with CH2Cl2 (10 mL), washed with sat. NH4Cl solution (2 x 20mL), sat. NaHCO3 solution (2 x20 mL), and the organic layer dried over Na2SO4 and concentrated to dryness. Purification wasperformed either by typical silica gel flash chromatography or preparative HPLC affording the desired-lactam carbamates.
According to the analysis of related databases, 171623-29-3, the application of this compound in the production field has become more and more popular.
Reference:
Article; Nuzzi, Andrea; Fiasella, Annalisa; Ortega, Jose Antonio; Pagliuca, Chiara; Ponzano, Stefano; Pizzirani, Daniela; Bertozzi, Sine Mandrup; Ottonello, Giuliana; Tarozzo, Glauco; Reggiani, Angelo; Bandiera, Tiziano; Bertozzi, Fabio; Piomelli, Daniele; European Journal of Medicinal Chemistry; vol. 111; (2016); p. 138 – 159;,
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