Bredikhina, Zemfira A. published the artcileFrom racemic epichlorohydrin to a single enantiomer of the drug timolol maleate, Computed Properties of 30165-97-0, the publication is Tetrahedron: Asymmetry (2015), 26(15-16), 797-801, database is CAplus.
The synthesis for a single enantiomer timolol maleate based on an initial Jacobsen hydrolytic kinetic resolution of racemic epichlorohydrin and on the stereochem. of the subsequent chem. transformations has been proposed. The feature of this synthesis is that both products of the kinetic resolution, (R)-epichlorohydrin and (S)-3-chloropropane-1,2-diol, have been utilized in the synthesis of the target, (S)-timolol (I). The mirror stereochem. results can be obtained with the use of (R,R)-salen Co(III) catalyst instead of (S,S)-salen Co(III).
Tetrahedron: Asymmetry published new progress about 30165-97-0. 30165-97-0 belongs to alcohols-buliding-blocks, auxiliary class Morpholine,Thiadiazole,Alcohol, name is 4-Morpholino-1,2,5-thiadiazol-3-ol, and the molecular formula is C6H9N3O2S, Computed Properties of 30165-97-0.
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