The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 14320-38-8, name is Cyclopent-3-enol. This compound has unique chemical properties. The synthetic route is as follows. COA of Formula: C5H8O
AddN-pyrimidinylpurine 1a (0.2 mmol), RhCl3?3H2O (0.004 mmol), Cu(OAc)2(0.4 mmol) andcyclopent-3-enol 2k (1.0 mmol) to 2.0 mL of DMF. , three times with carbon monoxide in the Young’s replacement tubeafter filling with carbon monoxide (1 atm), the reaction and after 90 deg.] C oil bath for 10 hours, the reaction was stopped until the reaction was cooled to roomtemperature, add ethyl acetate and saturated brine plurality Wash and extract.The organic phase was dried over anhydrous sodium sulfate and filtered.The solvent was evaporated to dryness, and ethyl acetate / petroleum ether (1:10 to 1:1) was purified by chromatography.The product was a whitesolid with a yield of 80%.
With the rapid development of chemical substances, we look forward to future research findings about 14320-38-8.
Reference:
Patent; Chinese Academy Of Sciences Lanzhou Chemical Physics Institute; Yang Lei; Zhao Kang; Liu Jianhua; Xia Chungu; Du Rongrong; (35 pag.)CN109851608; (2019); A;,
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