Extracurricular laboratory: Synthetic route of 112-70-9

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 112-70-9, 1-Tridecanol.

Synthetic Route of 112-70-9, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 112-70-9, name is 1-Tridecanol, molecular formula is C13H28O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.

General procedure: L-alanine esters were preparedaccording to a procedure reported earlier.5,6 Lalanine(1.0 mmol), 1-alcohol (1.0 mmol) and ptoluenesulphonicacid monohydrate (1.2 mmol) weretaken in about 30 mL of toluene and refluxed at 110C.After 5-6 h of refluxing, the solvent was removedby rotary evaporation under reduced pressure. Theresidue was dissolved in chloroform and washed with 10% sodium carbonate and then dried with anhydrous Na2SO4.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 112-70-9, 1-Tridecanol.

Reference:
Article; Sivaramakrishna; Swamy, Musti J.; Journal of Chemical Sciences; vol. 127; 9; (2015); p. 1627 – 1635;,
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