Related Products of 104-38-1, Adding some certain compound to certain chemical reactions, such as: 104-38-1, name is 1,4-Bis(2-hydroxyethoxy)benzene,molecular formula is C10H14O4, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 104-38-1.
A solution of 4-bis(2-hydroxyethoxy) benzene (6.0 g 30 mmol) and triphenylphosphine (18.9 g,72.1 mmol) in dry acetonitrile (200 mL) was cooled with an ice bath. Under vigorous stirring, carbon tetrabromide (24.0 g, 72.4 mmol) was slowly added. The mixture was stirred at room temperature for 12 hours. Then cold water (200 mL) was added to the reaction mixture to give white precipitation. The precipitate was collected, washed with methanol/water (3:2, 3 ¡Á 100 mL), recrystallized from methanol, and dried under vacuum to afford 1 as white crystals, 82.7% (14.5 g, 24.8mmol).
According to the analysis of related databases, 104-38-1, the application of this compound in the production field has become more and more popular.
Reference:
Article; Xiao, Xue-Dong; Bai, Ya-Li; Liu, Jia-Qi; Wang, Jun-Wen; Tetrahedron Letters; vol. 57; 30; (2016); p. 3385 – 3388;,
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