Tris(tetrabutylammonium) hexakis(tert-butanethiolato-κS)hepta-μ3-chlorido-μ3-sulfidohexamolybdate dihydrate was written by Petrov, Pavel A.;Naumov, Dmitry Yu.;Konchenko, Sergey N.. And the article was included in Acta Crystallographica, Section E: Structure Reports Online in 2012.Quality Control of Sodium 2-methyl-2-propanethiolate This article mentions the following:
The octahedral cluster core of the anion in the structure of the title compound, (C16H36N)3[Mo6(C4H9S)6(μ3-Cl)7(μ3-S)]·2H2O, has 3̅ site symmetry. Two μ3-Cl atoms fully occupy positions in the cluster core, while the remaining six positions are statistically occupied by Cl and S atoms in a 1:5 ratio. The fully occupied Cl-atom positions are located on sites with 3 symmetry, and the N atom of tetrabutylammonium cation is located on a site with 2 symmetry. The structure contains also two disordered solvent H2O mols., one of which is located on a 3-fold rotation axis and the other in a general position, both with an occupancy of 0.25. The H2O mols. are localized in cavities formed by the tetrabutylammonium cations and the tert-butanethiolate groups. The metal clusters are stacked in a cubic close packing arrangement along [001]. Crystallog. data and at. coordinates are given. In the experiment, the researchers used many compounds, for example, Sodium 2-methyl-2-propanethiolate (cas: 29364-29-2Quality Control of Sodium 2-methyl-2-propanethiolate).
Sodium 2-methyl-2-propanethiolate (cas: 29364-29-2) belongs to alcohols. Alcohols are weak acids. The most acidic simple alcohols (methanol and ethanol) are about as acidic as water, and most other alcohols are somewhat less acidic. A multistep synthesis may use Grignard-like reactions to form an alcohol with the desired carbon structure, followed by reactions to convert the hydroxyl group of the alcohol to the desired functionality.Quality Control of Sodium 2-methyl-2-propanethiolate
Referemce:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts