On September 7, 2021, Pan, Dandan; Xu, Shasha; Tian, Qingqiang; Li, Yahui published an article.Synthetic Route of 143-10-2 The title of the article was Pd-Catalyzed Intermolecular Transthiolation of Ar-OTf Using Methyl 3-(Methylthio) Propanoate as a Thiol Surrogate. And the article contained the following:
A method for the odorless synthesis of unsym. sulfides ArSR1 [Ar = naphth-1-yl, 3-NCC6H4, 4-F3CSC6H4, etc.; R1 = Me, Bn, CH2CH2Ph, etc.] via Csp2-O and Csp3-S bond activation was presented. Using Me 3-(methylthio) propanoate as a MeSH surrogate, a series of substituted aryl Me sulfides have been obtained in moderate to good yields. This catalytic protocol could also tolerated Me 3-(methylthio)propionate derivatives to afford the corresponding aryl sulfides. The experimental process involved the reaction of 1-Decanethiol(cas: 143-10-2).Synthetic Route of 143-10-2
The Article related to aryl sulfide preparation, triflate aryl methyl methylthio propanoate intermol transthiolation palladium catalyst, Benzene, Its Derivatives, and Condensed Benzenoid Compounds: Ethers, Sulfides, and The Corresponding Onium Compounds and other aspects.Synthetic Route of 143-10-2
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