Synthetic Route of C6H15NOIn 2021 ,《Semi-Interpenetrating Polymer Network Electrolytes Based on a Spiro-Twisted Benzoxazine for All-Solid-State Lithium-Ion Batteries》 appeared in ACS Applied Energy Materials. The author of the article were Lee, Jen-Yu; Yu, Tsung-Yu; Chung, Pei-Hsuan; Lee, Wen-Ya; Yeh, Shih-Chieh; Wu, Nae-Lih; Jeng, Ru-Jong. The article conveys some information:
A spiro-twisted benzoxazine, namely, 6,6′-(6,6,6′,6′-tetramethyl-6,6′,7,7′-tetrahydro-2H,2′H-8,8′-spirobi[indeno[5,6-e][1,3]oxazin]-3,3′(4H,4′H)-diyl)bis(hexan-1-ol) (TSBZ6D), was successfully developed as a semi-interpenetrating polymer network (s-IPN) matrix for solid polymer electrolytes (SPEs). The designed spiro-twisted mol. structure of TSBZ6D constitutes an SPE matrix with a high fractional free volume that facilitates the transport of lithium ions. In the meantime, its crosslinking network structure enables a remarkable enhancement in the mech. properties of SPEs. When combined with poly(ethylene oxide) (PEO) electrolytes, the TSBZ6D s-IPN imparts an enhancement of >300 and 1100% in tensile stress and in tensile strain, resp., to the PEO-TSBZ6D (PT) composite SPEs over the PEO/lithium salt sample. Electrochem. testing of sym. Li/PT/Li cells indicates the effectiveness of PT SPEs in mitigating the short-circuiting problem caused by Li dendrite formation. We demonstrated that a specific capacity of 166 mAh g-1 (0.1 C) at 80 °C and a promising cycle stability have been achieved by an all-solid-state LiFePO4/PT/Li. The experimental process involved the reaction of 6-Aminohexan-1-ol(cas: 4048-33-3Synthetic Route of C6H15NO)
6-Aminohexan-1-ol(cas: 4048-33-3) can undergo cyclization over copper supported on γ-alumina and magnesia to form hexahydro-1H-azepine. It may be used along with glutaric acid to generate poly(ester amide)s with excellent film- and fiber forming properties.Synthetic Route of C6H15NO
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