Tag: M.W=100-150

An article How high-resolution mass spectrometry can help for the accurate quantification of difficult fragrance allergens WOS:000592008400001 published article about 2-DIMENSIONAL GAS-CHROMATOGRAPHY; SOLID-PHASE DISPERSION; GC-MS QUANTIFICATION; SUSPECTED ALLERGENS; QUANTITATIVE-ANALYSIS; VOLATILE COMPOUNDS; DYNAMIC HEADSPACE; SCENTED TOYS; VALIDATION; PRODUCTS in [Remy, Pierre-Alain; Peres, Christophe; Corbi, Elise; David, Nathalie] Chanel, Lab Rech & Anal, 135 Ave Charles de Gaulle, F-92200 Neuilly Sur Seine, France; [Remy, Pierre-Alain; Dugay, Jose; Vial, Jerome] PSL Res Univ, ESPCI Paris, LSABM, CBI,CNRS,UMR 8231, Paris, France in 2021, Cited 53. Product Details of 105-13-5. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5

Two high-resolution mass spectrometers (HRMS) with different analyzer technology, Orbitrap and hybrid quadrupole time-of-flight (QTOF), were compared with a low-resolution mass spectrometer, quadrupole, to analyse a set of 35 difficult allergens. These difficult allergens are commonly coeluted fragrance allergens with matrix compounds, using standard gas chromatography-mass spectrometer conditions, from the extended list of the Scientific Committee on Consumer Safety (SCCS). Although the fundamental role of chromatographic separation has been demonstrated many times, the aim of this work is to demonstrate the benefits of high-resolution. The added value of high-resolution was illustrated in both a qualitative and a quantitative way. For qualitative aspect, the high resolution extracted ion signals of these two detectors were compared with the low-resolution extracted ion signals. About 50% of the coeluted cases observed with the low-resolution detector are easily resolved by the two high-resolution detectors. For the quantitative aspect, an accuracy profile methodology and a performance metric were used to propose an overall evaluation. The Orbitrap mass spectrometer demonstrated a better overall performance, while the QTOF presented similar or even lower quantification performances than the quadrupole on the set of analysed fragrances.

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Category: alcohols-buliding-blocks. In 2021 EUR J ORG CHEM published article about CATALYZED AEROBIC DEHYDROGENATION; BIOLOGICAL EVALUATION; MOLECULAR-OXYGEN; HECK REACTION; 2′-AMINOCHALCONES; EFFICIENT; FLAVANONES; INHIBITORS; CHEMISTRY; QUINOLONE in [Kim, Young Min; Yoo, Hyung-Seok; Son, Seung Hwan; Kim, Ga Yeong; Jang, Hyu Jeong; Kim, Dong Hwan; Kim, Nam-Jung] Kyung Hee Univ, Coll Pharm, 26 Kyungheedae Ro, Seoul 02447, South Korea; [Kim, Soo Dong; Park, Boyoung Y.; Kim, Nam-Jung] Kyung Hee Univ, Dept Life & Nanopharmaceut Sci, 26 Kyungheedae Ro, Seoul 02447, South Korea in 2021, Cited 36. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5.

2-Aryl-2,3-dihydroquinolin-4(1H)-ones have recently been identified as important structures with potent biological activities such as antitumor and antidiabetic effect. Herein, a total of 25 novel N-Tf 2-aryl-2,3-dihydroquinolin-4(1H)-ones were expediently synthesized via the oxidative aza-Michael cyclization of N-Tf-2 ‘-aminodihydrochalcones by ligand-free palladium(II) catalysis. This study presents a new synthetic approach to yield N-Tf 2-aryl-2,3-dihydroquinolin-4(1H)-ones, which can be easily transformed into pharmacologically interesting aza-flavanones and other N-heterocycles, such as quinolines and tetrahydroquinolines, in yields up to 84 %. This methodology has various advantages, which includes short reaction times under mild conditions and suitable functional group tolerance. Furthermore, a plausible mechanism was proposed and demonstrated by kinetic analysis.

Category: alcohols-buliding-blocks. Welcome to talk about 105-13-5, If you have any questions, you can contact Kim, YM; Yoo, HS; Son, SH; Kim, GY; Jang, HJ; Kim, DH; Kim, SD; Park, BY; Kim, NJ or send Email.

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Application In Synthesis of (4-Methoxyphenyl)methanol. Ou, W; Xiang, XD; Zou, R; Xu, Q; Loh, KP; Su, CL in [Ou, Wei; Xiang, Xudong; Zou, Ru; Su, Chenliang] Shenzhen Univ, Int Collaborat Lab 2D Mat Optoelect Sci & Technol, Engn Technol Res Ctr 2D Mat Informat Funct Device, Inst Microscale Optoelect, Shenzhen 518060, Peoples R China; [Xu, Qing] Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou, Zhejiang, Peoples R China; [Loh, Kian Ping] Natl Univ Singapore, Dept Chem, 3 Sci Dr 3, Singapore 117543, Singapore published Room-Temperature Palladium-Catalyzed Deuterogenolysis of Carbon Oxygen Bonds towards Deuterated Pharmaceuticals in 2021, Cited 50. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5.

Site-specific incorporation of deuterium into drug molecules to study and improve their biological properties is crucial for drug discovery and development. Herein, we describe a palladium-catalyzed room-temperature deuterogenolysis of carbon-oxygen bonds in alcohols and ketones with D-2 balloon for practical synthesis of deuterated pharmaceuticals and chemicals with benzyl-site (sp(3) C-H) D-incorporation. The highlights of this deoxygenative deuteration strategy are mild conditions, broad scope, practicability and high chemoselectivity. To enable the direct use of D2O, electrocatalytic D2O-splitting is adapted to in situ supply D-2 on demand. With this system, the precise incorporation of deuterium in the metabolic position (benzyl-site) of ibuprofen is demonstrated in a sustainable and practical way with D2O.

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In 2021 FRONT NEUROL published article about NEURAL-TUBE DEFECTS; PRIMARY CILIA; JOUBERT SYNDROME; GENE-EXPRESSION; MYOINOSITOL; MUTATIONS; PREVALENCE; REVEALS; GLUCOSE; ROLES in [Yue, Huixuan; Li, Shen; Qin, Jiaxing; Wang, Xiuwei; Guan, Zhen; Zhu, Zhiqiang; Niu, Bo; Guo, Jin; Wang, Jianhua] Capital Inst Pediat, Beijing Municipal Key Lab Child Dev & Nutr, Beijing, Peoples R China; [Yue, Huixuan; Li, Shen; Wang, Jianhua] Peking Union Med Coll, Grad Sch, Beijing, Peoples R China; [Gao, Tingting; Liu, Yu; Zhong, Rugang] Beijing Univ Technol, Coll Life Sci & Bioengn, Beijing Key Lab Environm & Viral Oncol, Beijing, Peoples R China; [Lyu, Jianjun] InnoStar BioTech Nantong Co Ltd, Dept Pathol, Nantong, Peoples R China in 2021, Cited 50. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5. Recommanded Product: 105-13-5

The inositol polyphosphate-5-phosphatase E (Inpp5e) gene is located on chromosome 9q34.3. The enzyme it encodes mainly hydrolyzes the 5-phosphate groups of phosphatidylinositol (3,4,5)-trisphosphate (PtdIns (3,4,5) P3) and phosphatidylinositol (4,5)-bisphosphate (PtdIns (4,5)P2), which are closely related to ciliogenesis and embryonic neurodevelopment, through mechanisms that are largely unknown. Here we studied the role of Inpp5e gene in ciliogenesis during embryonic neurodevelopment using inositol-deficiency neural tube defects (NTDs) mouse and cell models. Confocal microscopy and scanning electron microscope were used to examine the number and the length of primary cilia. The dynamic changes of Inpp5e expression in embryonic murine brain tissues were observed during Embryonic Day 10.5-13.5 (E 10.5-13.5). Immunohistochemistry, western blot, polymerase chain reaction (PCR) arrays were applied to detect the expression of Inpp5e and cilia-related genes of the embryonic brain tissues in inositol deficiency NTDs mouse. Real-time quantitative PCR (RT-qPCR) was used to validate the candidate genes in cell models. The levels of inositol and PtdIns(3,4) P2 were measured using gas chromatography-mass spectrometry (GC-MS) and enzyme linked immunosorbent assay (ELISA), respectively. Our results showed that the expression levels of Inpp5e gradually decreased in the forebrain tissues of the control embryos, but no stable trend was observed in the inositol deficiency NTDs embryos. Inpp5e expression in inositol deficiency NTDs embryos was significantly decreased compared with the control tissues. The expression levels of Inpp5e gene and the PtdIns (3,4) P2 levels were also significantly decreased in the inositol deficient cell model. A reduced number and length of primary cilia were observed in NIH3T3 cells when inositol deficient. Three important cilia-related genes (Ift80, Mkks, Smo) were down-regulated significantly in the inositol-deficient NTDs mouse and cell models, and Smo was highly involved in NTDs. In summary, these findings suggested that down-regulation of Inpp5e might be associated with abnormal ciliogenesis during embryonic neurodevelopment, under conditions of inositol deficiency.

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SDS of cas: 105-13-5. Authors Luo, NH; Zhong, YH; Wen, HL; Shui, HL; Luo, RS in WILEY-V C H VERLAG GMBH published article about in [Luo, Nianhua; Zhong, Yuhong; Wen, Huiling; Shui, Hongling; Luo, Renshi] Gannan Med Univ, Sch Pharmaceut Sci, Ganzhou 341000, Jiangxi, Peoples R China in 2021, Cited 94. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5

Ketones are of great importance in synthesis, biology, and pharmaceuticals. This paper reports an iridium complexes-catalyzed cross-coupling of alcohols via hydrogen borrowing, affording a series of alpha-alkylated ketones in high yield (86 %-95 %) and chemoselectivities (>99 : 1). This methodology has the advantages of low catalyst loading (0.1 mol%) and environmentally benign water as the solvent. Studies have shown the amount of base has a great impact on chemoselectivities. Meanwhile, deuteration experiments show water plays an important role in accelerating the reduction of the unsaturated ketones intermediates. Remarkably, a gram-scale experiment demonstrates this methodology of iridium-catalyzed cross-coupling of alcohols has potential application in the practical synthesis of alpha-alkylated ketones.

Welcome to talk about 105-13-5, If you have any questions, you can contact Luo, NH; Zhong, YH; Wen, HL; Shui, HL; Luo, RS or send Email.. SDS of cas: 105-13-5

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An article TEMPO-Functionalized Nanoreactors from Bottlebrush Copolymers for the Selective Oxidation of Alcohols in Water WOS:000664332300013 published article about FREE AEROBIC OXIDATION; SUPPORTED TEMPO; ASYMMETRIC SULFOXIDATION; BLOCK-COPOLYMERS; CATALYST; METAL; EFFICIENT; DEHYDROGENATION; ALDEHYDES in [Wang, Maolin; Xu, Zhenkai; Shi, Yi; Cai, Fang; Qiu, Jiaqi; Chen, Tao] Zhejiang Sci Tech Univ, Minist Educ, Key Lab Adv Text Mat & Mfg Technol, Hangzhou 310018, Peoples R China; [Wang, Maolin; Xu, Zhenkai; Shi, Yi; Cai, Fang; Qiu, Jiaqi; Chen, Tao] Zhejiang Sci Tech Univ, Minist Educ, Ecodyeing & Finishing Engn Res Ctr, Hangzhou 310018, Peoples R China; [Wang, Maolin; Xu, Zhenkai; Shi, Yi; Cai, Fang; Qiu, Jiaqi; Chen, Tao] Zhejiang Sci Tech Univ, Natl Base Int Sci & Technol Cooperat Text & Consu, Hangzhou 310018, Peoples R China; [Shi, Yi; Cai, Fang] Zhejiang Cady Ind Co Ltd, Huzhou 313013, Peoples R China; [Yang, Guang; Hua, Zan] Anhui Agr Univ, Biomass Mol Engn Ctr, Dept Mat Sci & Engn, Hefei 230036, Peoples R China in 2021, Cited 56. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5. Product Details of 105-13-5

Polymeric nanoreactors in water fabricated by the self-assembly of amphiphilic copolymers have attracted much attention due to their good catalytic performance without using organic solvents. However, the disassembly and instability of relevant nanostructures often compromise their potential applicability. Herein, the preparation of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO)-containing nanoreactors by the self-assembly of amphiphilic bottle-brush copolymers has been demonstrated. First, a macromonomer having a norbornenyl polymerizable group was prepared by RAFT polymerization of hydrophobic and hydrophilic monomers. The macromonomer was further subjected to ring-opening metathesis polymerization to produce an amphiphilic bottlebrush copolymer. Further, TEMPO, as a catalyst, was introduced into the hydrophobic block through the activated ester strategy. Finally, TEMPO-functionalized polymeric nanoreactors were successfully obtained by self-assembly in water. The nanoreactors exhibited excellent catalytic activities in selective oxidation of alcohols in water. More importantly, the reaction kinetics showed that the turnover frequency is greatly increased compared to that of the similar nanoreactor prepared from liner copolymers under the same conditions. The outstanding catalytic activities of the nanoreactors from bottlebrush copolymers could be attributed to the more stable micellar structure using the substrate concentration effect. This work presents a new strategy to fabricate stable nanoreactors, paving the way for highly efficient organic reactions in aqueous solutions.

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Category: alcohols-buliding-blocks. Authors Zhou, ZY; Xie, YN; Zhu, WZ; Zhao, HY; Yang, NJ; Zhao, GH in ELSEVIER published article about in [Zhou, Zhaoyu; Xie, Ya-Nan; Zhu, Wenze; Zhao, Hongying; Zhao, Guohua] Tongji Univ, Shanghai Tongji Hosp, Sch Chem Sci & Engn, Inst Translat Res, Shanghai 200092, Peoples R China; [Yang, Nianjun] Univ Siegen, Inst Mat Engn, D-57076 Siegen, Germany in 2021, Cited 55. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5

Hydrogen production can be promoted by replacing sluggish oxygen evolution reaction (OER) with a thermodynamically more favorable reaction, the primary oxidation reaction of benzyl alcohol to benzaldehyde. On a Bi2MoO6@TiO(2)NTA photocathode, the conversion of benzyl alcohol to benzaldehyde is realized with the selectivity of 100 %. This is originated from enhanced adsorption and activation of benzyl alcohol on this photoanode, as confirmed from tested by in situ FTIR techniques. The electrons generated during such a controllable and selective primary oxidation reaction is then utilized as the source for synergistical hydrogen production. The amount of generated hydrogen is then 5.5 times higher than that when OER is used. The efficiency for such hydrogen production is as high as 85 %. The proposed strategy combines solar energy and biomass for the efficient production of the valuable raw material – benzaldehyde as well as green energy source – hydrogen.

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Formula: C8H10O2. I found the field of Chemistry very interesting. Saw the article Magnetically recyclable CuFe2O4 catalyst for efficient synthesis of bis (indolyl)methanes using indoles and alcohols under mild condition published in 2021, Reprint Addresses Hung, TQ; Vu, XH (corresponding author), Vietnam Acad Sci & Technol, Inst Chem, 18 Hoang Quoc Viet, Hanoi, Vietnam.; Dang, TT (corresponding author), VNU Hanoi Univ Sci, Dept Chem, 19 Le Thanh Tong, Hanoi, Vietnam.; Vu, XH (corresponding author), Vietnam Petr Inst, 167 Trung Kinh Str, Hanoi, Vietnam.. The CAS is 105-13-5. Through research, I have a further understanding and discovery of (4-Methoxyphenyl)methanol.

Bis(3-indolyl)methanes (BIM) are highly valuable and appear in the core structure of many natural products and pharmacologically active compounds (anticancer, anti-inflammatory, antiobesity, antimetastatic, antimicrobial, etc.). Herein, we have disclosed an air stable and highly efficient CuFe2O4 heterogeneous catalyst for alkylation of indoles with alcohols to give bis(3-indolyl)methanes in very good yields. The CuFe2O4 catalyst has been found to be magnetically recycled at least five times without losing significant catalytic activity.

Formula: C8H10O2. Welcome to talk about 105-13-5, If you have any questions, you can contact Nguyen, NK; Ha, MT; Bui, HY; Trinh, QT; Tran, BN; Nguyen, VT; Hung, TQ; Dang, TT; Vu, XH or send Email.

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Authors Kargar, PG; Bagherzade, G; Eshghi, H in ROYAL SOC CHEMISTRY published article about ONE-POT SYNTHESIS; RECOVERABLE NANO-CATALYST; FACILE SYNTHESIS; IONIC LIQUID; RECYCLABLE CATALYST; NATURAL PHOSPHATE; HIGHLY EFFICIENT; GREEN CHEMISTRY; SULFONIC-ACID; NANOPARTICLES in [Kargar, Pouya Ghamari; Bagherzade, Ghodsieh] Univ Birjand, Fac Sci, Dept Chem, Birjand 97175615, Iran; [Eshghi, Hossein] Ferdowsi Univ Mashhad, Fac Sci, Dept Chem, Mashhad, Razavi Khorasan, Iran in 2021, Cited 77. SDS of cas: 105-13-5. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5

In this work, the new trinuclear manganese catalyst defined as Fe3O4@NFC@NNSM-Mn(iii) was successfully manufactured and fully characterized by different techniques, including FT-IR, XRD, TEM, SEM, EDX, VSM, and ICP analysis. There have been reports of the use of magnetic catalysts for the synthesis of xanthine derivatives. The critical potential interest in the present method include short reaction time, high yields, recyclability of the catalyst, easy workup, and the ability to sustain a variety of functional groups, which give economical as well as ecological rewards. Also, the synthesized catalyst was used as a recyclable trinuclear catalyst in alcohol oxidation reactions at 40 degrees C. The magnetic catalyst activity of Fe3O4@NFC@NNSM-Mn(iii) could be attributed to the synergistic effects of the catalyst Fe3O4@NFC@NNS-Mn(iii) with melamine. Employing a sustainable and safe low temperature, using an eco-friendly solvent, no need to use any additive, and long-term stability and magnetic recyclability of the catalyst for at least six successive runs are the advantages of the current protocol towards green chemistry. This protocol is a benign, environmentally friendly method for heterocycle synthesis.

SDS of cas: 105-13-5. Bye, fridends, I hope you can learn more about C8H10O2, If you have any questions, you can browse other blog as well. See you lster.

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An article 4-Aryl-1,4-Dihydropyridines as Potential Enoyl-Acyl Carrier Protein Reductase Inhibitors: Antitubercular Activity and Molecular Docking Study WOS:000629032900004 published article about BINDING MODE ANALYSIS; DIHYDROPYRIDINE DERIVATIVES; ANTIMOSQUITO PROPERTIES; MULTIDRUG-RESISTANT; LARVICIDAL ACTIVITY; INHA INHIBITORS; DESIGN; 1,4-DIHYDROPYRIDINES; POLYMORPHISM; DISCOVERY in [Venugopala, Katharigatta N.; Morsy, Mohamed A.; Aldhubiab, Bandar E.; Attimarad, Mahesh; Nair, Anroop B.; Sreeharsha, Nagaraja] King Faisal Univ, Coll Clin Pharm, Dept Pharmaceut Sci, Al Hasa 31982, Saudi Arabia; [Venugopala, Katharigatta N.; Mohanlall, Viresh] Durban Univ Technol, Dept Biotechnol & Food Technol, ZA-4001 Durban, South Africa; [Deb, Pran Kishore] Philadelphia Univ, Fac Pharm, Dept Pharmaceut Sci, Amman 19392, Jordan; [Pillay, Melendhran] Inkosi Albert Luthuli Cent Hosp, Dept Microbiol, Natl Hlth Lab Serv, KZN Acad Complex, ZA-4001 Durban, South Africa; [Chopra, Deepak] Indian Inst Sci Educ & Res Bhopal, Dept Chem, Bhopal By Pass Rd, Bhopal 462066, Madhya Pradesh, India; [Chandrashekharappa, Sandeep] GKVK, Inst Stem Cell Biol & Regenerat Med, TIFR, NCBS, Bangalore 560065, Karnataka, India; [Morsy, Mohamed A.] Menia Univ, Fac Med, Dept Pharmacol, El Minia 61511, Egypt; [Sreeharsha, Nagaraja] Vidya Siri Coll Pharm, Dept Pharmaceut, Off Sarjapura Rd, Bengaluru 560035, India; [Kandeel, Mahmoud] King Faisal Univ, Coll Vet Medi Cine, Dept Biomed Sci, Al Hasa 31982, Saudi Arabia; [Kandeel, Mahmoud] Kafrelsheikh Univ, Fac Vet Med, Dept Pharmacol, Kafrelsheikh 33516, Egypt; [Venugopala, Rashmi] Univ KwaZulu Natal, Dept Publ Hlth Med, Howard Coll Campus, ZA-4001 Durban, South Africa in 2021, Cited 93. The Name is (4-Methoxyphenyl)methanol. Through research, I have a further understanding and discovery of 105-13-5. Recommanded Product: 105-13-5

Background: Tuberculosis remains one of the most deadly infectious diseases worldwide due to the emergence of multi-drug resistance (MDR) and extensively drug resistance (XDR) strains of Mycobacterium tuberculosis (MTB). Aims: Currently, available drugs are getting resistant and toxic. Hence, there is an urgent need for the development of potent molecules to treat tuberculosis. Materials and Methods: Herein, the screening of a total of eight symmetrical 1,4-dihydropyridine (1,4-DHP) derivatives (4a-4h) was carried out for whole-cell anti-TB activity against the susceptible H37Rv and MDR strains of MTB. Results and Discussion: Most of the compounds exhibited moderate to excellent activity against the susceptible H37Rv. Moreover, the most promising compound 4f (against H37Rv) having para-trifluoromethyl phenyl group at 4-position and bis para-methoxy benzyl ester group at 3- and 5-positions of 1,4- dihydropyridine pharmacophore, exhibited no toxicity, but demonstrated weak activity against MTB strains resistant to isoniazid and rifampicin. In light of the inhibitory profile of the title compounds, enoyl-acyl carrier protein reductase (InhA) appeared to be the appropriate molecular target. A docking study of these derivatives against InhA receptor revealed favorable binding interactions. Further, in silico predicted ADME properties of these compounds 4a-4h were found to be in the acceptable ranges, including satisfactory Lipinski’s rule of five, thereby indicating their potential as drug-like molecules. Conclusion: In particular, the 1,4-DHP derivative 4f can be considered an attractive lead molecule for further exploration and development of more potent anti-TB agents as InhA inhibitors.

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